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on 2018-1-17
00:00 UTC / 09:00 JST
Summary Structural Experimental Function Sequence Neighbor History Download Link

Mine: 4tmcCRYSTAL STRUCTURE of OLD YELLOW ENZYME from CANDIDA MACEDONIENSIS AKU4588 COMPLEXED with P-HYDROXYBENZALDEHYDE

Experimental method : X-RAY DIFFRACTION

Refinement Statistics

Cell axes [Å]52.394151.027199.893
Cell angles [degree]90.0090.0090.00
SpacegroupP 21 21 21
Resolution limits [Å] (low - high) 19.95 - 1.80
the highest resolution shell value 1.85 - 1.80
R-work0.167
the highest resolution shell value 0.2200
R-free0.205
the highest resolution shell value 0.2610
RMSD bond length [Å]0.018
RMSD bond angle [degree]1.892

Data Collection Statistics

Resolution limits [Å] (low - high) 20.000 - 1.800
Number of reflections147656
Number of measurements 
Rmerge_I_obs 
Completeness [%]99.9
Redundancy7.3

Crystallization Conditions

crystal IDmethodpHpH rangetemparatureunit
1VAPOR DIFFUSION, SITTING DROP8.08.0293 


        


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